HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21709913, compound → HCID 21709932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21709913 | HCID 21709913 | — |
| Reactant | HCID 178518971 | HCID 178518971 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 21709932 | HCID 21709932 | — |
Reaction Steps
Similarly to the process described in Example 1, 2.5 g (10 mmol) of 1-(2-bromophenyl)-1,2-dihydro-5H-tetrazol-5-one, 2 g (10 mmol) of N-methyl-N-(tetrahydro-2H-thiopyran-4-yl)carbamoyl chloride and 1.5 g (12 mmol) of 4-dimethylaminopyridine were reacted. Yield 2.5 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277790B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-7b40b2bb5e034993b8a28ed5d0d229af |
| Source note | uspto-grants-2001_08 |