HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl 2-iodo-3-methoxybenzoate → methyl 2',6-dimethoxybiphenyl-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl 2-iodo-3-methoxybenzoate | HCID 299486 | — |
| Reactant | 2-Methoxyphenylboronic acid | HCID 2733958 | — |
| Product | methyl 2',6-dimethoxybiphenyl-2-carboxylate | HCID 282428 | — |
Reaction Steps
Using the procedure outlined in Step A of Example 18, 201.7 mg (0.69 mmol) of methyl-2-iodo-3-methoxy-benzoate and 125.9 mg (0.82 mmol) of 2-methoxy-phenylboronic acid gave after 27 hours of reflux a quantitative yield of the title substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277843B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-b9779ce725614451a9787927c946bbc3 |
| Source note | uspto-grants-2001_08 |