HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 21710215, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Hydroxybenzonitrile | HCID 11907 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21710215 | HCID 21710215 | — |
Reaction Steps
Potassium carbonate (30 mmol) and then ethyl acetate (11 mmol) are added to a solution of 2-hydroxybenzonitrile (10 mmol) in acetonitrile. After stirring overnight, the solution is filtered and evaporated, the residue is taken up in ethyl acetate, and the organic phase is washed, dried and then evaporated to yield the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277851B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-37dafa11ed444634bf7101b15c2d34fd |
| Source note | uspto-grants-2001_08 |