HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13714726, compound → HCID 13714728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13714726 | HCID 13714726 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13714728 | HCID 13714728 | 97.2% |
Reaction Steps
4.78 g of alpha-isopropyl-alpha-[3-[N-[3-(2-nitrophenoxy)propyl]amino]propyl]-3,4,5-trimethoxyphenyl-acetonitrile was hydrogenated in 100 ml of methanol over 50 mg of platinum oxide at atmospheric pressure and room temperature. The catalyst was filtered off and filtrate was evaporated to give 4.36 g of desired compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04612329 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-0def383bcd52460d8c89ff77202dcd60 |
| Source note | uspto-grants-1986_09 |