HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 7-Amino-2-methyl-3,4-dihydroisoquinolinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3,4-Dihydroisoquinolin-7-amine | HCID 11423667 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 7-Amino-2-methyl-3,4-dihydroisoquinolinium iodide | HCID 11108962 | — |
Reaction Steps
7-amino-3,4-dihydroisoquinoline (0.40 g, 2.74 mmol) in acetone (125 ml) was treated with iodomethane (0.50 ml, 8.03 mmol) and left stirring at room temperature for 18 h. The resultant yellow precipitate was collected by filtration and dried in vacuo at ambient temperature (0.73 g, 92%). m/z (API)=161 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277861B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-a31009c6874141d691607b362acda856 |
| Source note | uspto-grants-2001_08 |