HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13714730, compound → HCID 13714732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13714730 | HCID 13714730 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13714732 | HCID 13714732 | 105.2% |
Reaction Steps
0.92 g of alpha-isopropyl-alpha-[3-[N-[3-(2-nitrophenoxy)propyl]-N-methylamino]propyl]-3,4,5-trimethoxyphenylacetonitrile was hydrogenated in 20 ml of methanol over 10 mg of platinum oxide at atmospheric pressure and room temperature. The catalyst was filtered off and filtrate was evaporated to give 0.91 g of the desired compound as a yellow oil. The oxalate of this compound was obtained in the usual manner.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04612329 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-2f0e8264333b4780b3d6f70d45b41568 |
| Source note | uspto-grants-1986_09 |