HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21710574, compound → HCID 21710568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21710574 | HCID 21710574 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21710568 | HCID 21710568 | 92% |
Reaction Steps
A solution of the product from Example 19B (1.07 g, 5.19 mmol) was reduced using hydrogen gas at 4 atm in the presence of Rh/alumina in methanol to provide 1.02 g (92%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277871B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-70bfd030a2584546bb7a157fd65ea689 |
| Source note | uspto-grants-2001_08 |