HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 651131Generated: November 1, 2026
1,4-Dioxane hydrochloride → HCID 66548467, compound
https://huagongshe.com/reaction/651131
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 52530575 | HCID 52530575 | — |
| Product | HCID 66548467 | HCID 66548467 | — |
Reaction Steps
(S)-(1-Benzyl-2-oxo-2-thiomorpholin-4-yl-ethyl)-carbamic acid tert-butyl ester (17.8 mmol) was dissolved in 4M HCl-dioxane (67 mL) at 0° C., the solution stirred at 25° C. for 1 hour, the reaction concentrated and the residue triturated with ether. Yield, 5.0 g, 98%; PBMS 251 (MH+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06277877B1 |
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| Source dataset | uspto-grants-2001_08 |
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| ORD ID | ord-53f00d2017fb4ab084c5532420902580 |
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| Source note | uspto-grants-2001_08 |
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