HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 651153Generated: November 1, 2026
HCID 7201349, compound → HCID 13689667, compound
https://huagongshe.com/reaction/651153
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 7201349 | HCID 7201349 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 13689667 | HCID 13689667 | — |
Reaction Steps
(R)-(1-Methylcarbamoyl-2-phenyl-ethyl)-carbamic acid tert-butyl ester (722 mg, 2.6 mmol) was dissolved in 4M HCl-dioxane (10 mL) at 0° C. The mixture was stirred for 1 hour at 25° C., concentrated and the residue triturated with ether. Yield, 517 mg, 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06277877B1 |
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| Source dataset | uspto-grants-2001_08 |
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| ORD ID | ord-e3880eb35d8f4dcca92489751a8cb03b |
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| Source note | uspto-grants-2001_08 |
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