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HRID651306

反应详情

EQUATION

反应方程式

HRID 651306 的结构方程式

REACTANTS

反应物

3
结构：BrBr
HCID24408

Bromine

Br2

结构：CCCCCC[C@@H](C)Oc1ccccc1C#N
HCID21308782

未命名化合物

结构：CC[C@H](C)COc1ccc(Br)cc1C#N
HCID53787839

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCC[C@@H](C)Oc1ccc(Br)cc1C#N
HCID53905579

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

Quantities: compound 40 (12.34 g, 0.054 mol), bromine (17.15 g, 0.0107 mol), chloroform (100 ml). The experimental procedure was as described for the preparation of compound 41. The crude product was purified by column chromatography (20% petrol/dichloromethane) to give a fawn oil.

WORKUP

后处理

  1. customThe crude product was purified by column chromatography (20% petrol/dichloromethane)
  2. customto give a fawn oil