HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Azaindole → HCID 54447290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Azaindole | HCID 9220 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Product | HCID 54447290 | HCID 54447290 | — |
Reaction Steps
The title compound is prepared from 1H-pyrrolo[3,2-c]pyridine as described in EXAMPLES 18 and 19, Part A using tert-butyl bromoacetate in place of methyl iodide. The crude product is purified by column chromatography eluting with a gradient of 3% MeOH/CH2Cl2 to 6% MeOH/CH2Cl2 to give the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06281227B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-b83882fafd474bdaa10245e91d475de6 |
| Source note | uspto-grants-2001_08 |