HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(Diphenylmethyl)methylamine → Methyl (n-diphenylmethyl-n-methylsulfamoyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(Diphenylmethyl)methylamine | HCID 411467 | — |
| Reactant | Methyl (chlorosulfonyl)acetate | HCID 11435213 | — |
| Product | Methyl (n-diphenylmethyl-n-methylsulfamoyl)acetate | HCID 20681419 | 37% |
Reaction Steps
The subtitle compound (3.05 g, 37%) was prepared as a clear brown oil from N-methyl benzhydrylamine (prepared according to the method of Z. Horii, T Sakai and Inoi, Pharm Bull., 1955, 3, 159) (10.7 g, 50.7 mmol) and methyl chlorosulfonylacetate (4.27 g, 24.7 mmol), using the method of Example 1(a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06281357B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-94b65b19089241e7b12f702a48d48957 |
| Source note | uspto-grants-2001_08 |