HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → (n-Diphenylmethyl-n-methylsulfamoyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl (n-diphenylmethyl-n-methylsulfamoyl)acetate | HCID 20681419 | — |
| Product | (n-Diphenylmethyl-n-methylsulfamoyl)acetamide | HCID 21709118 | 90% |
Reaction Steps
The subtitle compound (2.62 g, 90%) was prepared as a white solid from aqueous ammonia solution (10 ml, s.g.=0.88) and methyl (N-diphenylmethyl-N-methylsulfamoyl)acetate (from step (a), 3.05 g, 9.2 mmol), using the method of Example 1(b). m.p. 110-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06281357B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-43f16bb76df34dcca17e4b167d7544a3 |
| Source note | uspto-grants-2001_08 |