Ammonia → HCID 21709115, compound

HRID 651711Notes

Reaction equation

HRID 651711 reaction equation
C[O:2][C:3](=O)[CH2:4][S:5](=[O:13])(=[O:12])[N:6]([C:8]([CH3:11])([CH3:10])[CH3:9])[CH3:7].[NH3:15]>>[C:8]([N:6]([CH3:7])[S:5]([CH2:4][C:3]([NH2:15])=[O:2])(=[O:13])=[O:12])([CH3:11])([CH3:10])[CH3:9]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 21709104HCID 21709104, compound

Product 1

HCID 21709115HCID 21709115, compoundYield 84%

Procedure

The subtitle compound (3.66 g, 84%) was prepared as a white solid from aqueous ammonia solution (10 ml, s.g.=0.88) and methyl (N-tert-butyl-N-methylsulfamoyl)acetate (from step (a), 4.7 g, 21 mmol), using the method of Example 1(b). m.p. 105-109° C.

Sources & evidence

ORD record
ord-14d4faf22627487a83ad5da2357b9049
Source dataset
uspto-grants-2001_08
Patent number
US06281357B1

Reaction notes

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