HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 21709115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 21709104 | HCID 21709104 | — |
| Product | HCID 21709115 | HCID 21709115 | 84% |
Reaction Steps
The subtitle compound (3.66 g, 84%) was prepared as a white solid from aqueous ammonia solution (10 ml, s.g.=0.88) and methyl (N-tert-butyl-N-methylsulfamoyl)acetate (from step (a), 4.7 g, 21 mmol), using the method of Example 1(b). m.p. 105-109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06281357B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-14d4faf22627487a83ad5da2357b9049 |
| Source note | uspto-grants-2001_08 |