HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 135626360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 135626364 | HCID 135626364 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 135626360 | HCID 135626360 | — |
Reaction Steps
To a solution of N-cyclohexyl-N-(2-acetoxyethyl)-4-(2-oxo-3-methylene-1,2,3,5-tetrahydroimidazo[2,1-b]quinazolin-7-yl)oxybutanamide 50 mg in ethanol (20 ml) was added 3N NaOH (5 ml) in small portions. After 30 minutes at room temperature, the reaction mixture was neutralized with concentrated HCl and the resulting precipitate was collected by filtration and dried to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670434 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-ceb7fe28475348d2a651bc4c8f519518 |
| Source note | uspto-grants-1987_06 |