HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidin-4-ol → 6-(2-Chlorophenyl)-3-(4-hydroxypiperidino)-1,2,4-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidin-4-ol | HCID 79341 | — |
| Reactant | 3-Chloro-6-(o-chlorophenyl)-1,2,4-triazine | HCID 12581288 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-(2-Chlorophenyl)-3-(4-hydroxypiperidino)-1,2,4-triazine | HCID 13605526 | — |
Reaction Steps
7.4 g of 3-chloro-6-(2-chlorophenyl)-1,2,4-triazine, prepared according to J. Het. Chem. 16, 1402 (1979), and 9 g of 4-hydroxypiperidine are heated under reflux in 150 ml of ethanol for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04613603 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-9445a3bf9c0f4684960d69b700f0cd72 |
| Source note | uspto-grants-1986_09 |