HRID652020

反应详情

EQUATION

反应方程式

HRID 652020 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a stirred, hot solution of 4.5 g. 4-[14-(trimethylsilyl)tetradecylamino]benzoic acid in 150 ml. absolute ethanol was added 2.2 ml. 10N sodium hydroxide. The solution was cooled and the precipitate was filtered off and dried to yield a light yellow solid, m.p. 350°-355° C. dec.

WORKUP

后处理

  1. temperatureThe solution was cooled
  2. filtrationthe precipitate was filtered off
  3. customdried
  4. customto yield a light yellow solid, m.p. 350°-355° C. dec.