HRID652020
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a stirred, hot solution of 4.5 g. 4-[14-(trimethylsilyl)tetradecylamino]benzoic acid in 150 ml. absolute ethanol was added 2.2 ml. 10N sodium hydroxide. The solution was cooled and the precipitate was filtered off and dried to yield a light yellow solid, m.p. 350°-355° C. dec.
WORKUP
后处理
- temperatureThe solution was cooled
- filtrationthe precipitate was filtered off
- customdried
- customto yield a light yellow solid, m.p. 350°-355° C. dec.