HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Sodium 4-[14-(trimethylsilyl)tetradecylamino]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-[14-(Trimethylsilyl)tetradecylamino)benzoic acid | HCID 13884862 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Sodium 4-[14-(trimethylsilyl)tetradecylamino]benzoate | HCID 23702177 | — |
Reaction Steps
To a stirred, hot solution of 4.5 g. 4-[14-(trimethylsilyl)tetradecylamino]benzoic acid in 150 ml. absolute ethanol was added 2.2 ml. 10N sodium hydroxide. The solution was cooled and the precipitate was filtered off and dried to yield a light yellow solid, m.p. 350°-355° C. dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670421 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-2645a447203f4c6596900cf4364ac758 |
| Source note | uspto-grants-1987_06 |