HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20199126, compound → HCID 178472251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20199126 | HCID 20199126 | — |
| Reactant | HCID 54510571 | HCID 54510571 | — |
| Product | HCID 178472251 | HCID 178472251 | 155.6% |
Reaction Steps
A mixture of 3-[3-(1-piperidinylmethyl)phenoxy]propanamine (A) (3.61 g) and ethyl 3-[[[1-methyl-2-(phenylmethylene)hydrazino](methylthio)methylene]amino]-3-oxopropanoate (4.7 g) was heated at 50° under water pump vacuum during 4 h. to gave the title compound as an orange gum (7.3 g). T.l.c. System D, Rf 0.65.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670448 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-ddf84ac8e9ba4d7e84d51bdfb7ad6095 |
| Source note | uspto-grants-1987_06 |