HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 14032620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 178435995 | HCID 178435995 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14032620 | HCID 14032620 | 51% |
Reaction Steps
A mixture of 1.6 g of 3-(1-pheneth-2-yl-4-piperidinyl)-1H-indazole and 7 ml of benzoyl chloride was heated at 100° for 2 hr. After cooling, ether was added and the solid was collected. The solid was combined with material from a prior experiment and recrystallized from methanol to yield 2.4 g (51%) of product, mp 248°-250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670447 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-e9032a7800fe4848a1da2888e96a8934 |
| Source note | uspto-grants-1987_06 |