HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 652149Generated: October 28, 2026
Benzoyl chloride, 3-chloro- → HCID 14032531, compound
https://huagongshe.com/reaction/652149
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Reactant | HCID 178480237 | HCID 178480237 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14032531 | HCID 14032531 | 67.7% |
Reaction Steps
A mixture of 3.0 g of 3-(1-methyl-4-piperidinyl)-1H-indazole and 8 ml of 3-chlorobenzoyl chloride was heated at 100° C. for 2 hours. The reaction was allowed to cool, and ether was added. The resultant solid was collected and recrystallized twice from isopropyl alcohol to yield 3.7 g (67.7%) of product, mp 209°-211° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04670447 |
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| Source dataset | uspto-grants-1987_06 |
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| ORD ID | ord-b51d5c263cfe4678acea74e2b3c386a7 |
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| Source note | uspto-grants-1987_06 |
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