HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → 4-tert-Butyl-2,6-diethylmorpholin-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 1,2-Epoxybutane | HCID 7834 | — |
| Product | 4-tert-Butyl-2,6-diethylmorpholin-2-ol | HCID 20199606 | 61% |
| Product | HCID 23423723 | HCID 23423723 | 30% |
Reaction Steps
tert-Butylamine (17.0 g, 0.23 mol) and 1,2-epoxybutane (50 g, 0.69 mol) were subjected to a reaction as described in Example 1 above. A 61% yield of 4-tert-butyl-2,6-diethyl-2-hydroxymorpholine was obtained along with a 30% yield of N-tert-butyl-bis-(2-hydroxybutyl)amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670557 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-931f1536f6e746029d623b4272d786fa |
| Source note | uspto-grants-1987_06 |