HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → 2-Cyclopropyl-4-methoxy-6-(trichloromethyl)-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 2-Cyclopropyl-4,6-bis-trichloromethyl-1,3,5-triazine | HCID 20199613 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Cyclopropyl-4-methoxy-6-(trichloromethyl)-1,3,5-triazine | HCID 20199618 | — |
Reaction Steps
To a solution of 48 g of 2-cyclopropyl-4,6-bis-(trichloromethyl)-1,3,5-triazine in 200 ml of MeOH are added, with stirring, 4.9 g of sodium methylate, and the mixture is stirred for 1 hour at room temperature; it is then filtered and the filtrate is evaporated to dryness. The yield is 28.5 g of the title compound as a light-red oil, which solidifies after some time, m.p. 49°-51° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670559 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-16fb1c70e63e4e61be89e234bb424404 |
| Source note | uspto-grants-1987_06 |