HCID 13930814, compound → MLS000757167

HRID 652286Notes

Reaction equation

HRID 652286 reaction equation
C([O:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[CH:21]=[CH:20][C:19]([C:22](=[O:29])[C:23]3[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=3)=[CH:18][CH:17]=2)=[CH:12][CH:11]=1)(=O)C1C=CC=CC=1>O1CCCC1>[OH:9][C:10]1[CH:11]=[CH:12][C:13]([C:16]2[CH:21]=[CH:20][C:19]([C:22](=[O:29])[C:23]3[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=3)=[CH:18][CH:17]=2)=[CH:14][CH:15]=1

Participants

3

Reactant 1

HCID 13930814HCID 13930814, compound2×

Product 1

HCID 344075MLS000757167

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

4-Benzoyloxy-4'-benzoylbiphenyl [compound (11)] in Example 12 was added to an alkali-containing tetrahydrofuran followed by stirring at room temperature for several hours. After completion of the reaction, the tetrahydrofuran solution was concentrated to obtain 4-hydroxy-4'-benzoylbiphenyl [compound (31)]. The results are shown in Table 8.

Workup

  1. customAfter completion of the reaction
  2. concentrationthe tetrahydrofuran solution was concentrated

Sources & evidence

ORD record
ord-c333fb50279e4b1b99496322e189f378
Source dataset
uspto-grants-1987_06
Patent number
US04670581

Reaction notes

Loading…