関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Lauroyl peroxide | HCID 7773 | — |
| 反応物 | Vinyl Acetate | HCID 7904 | — |
| 反応物 | Maleic Anhydride | HCID 7923 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | Acetic acid ethenyl ester, polymer with 2,5-furandione | HCID 269112 | — |
反応手順
13 g (0.5 mole) of vinyl acetate, 49 g (0.5 mole) of maleic acid anhydride and 0.1 g of lauroyl peroxide were dissolved in 400 cc of benzene and heated for five hours at 70° C. The copolymer was precipitated from the viscous solution with petroleum ether (80° to 100° C.). The copolymer dissolved well in diluted caustic soda.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04671982 |
|---|
| 出典データセット | uspto-grants-1987_06 |
|---|
| ORD ID | ord-a8ca235c9ca844d4bdd9af51edf5e228 |
|---|
| 出典メモ | uspto-grants-1987_06 |
|---|
