1-Bromo-3-chloropropane → HCID 13808542, compound

HRID 652434Notes

Reaction equation

HRID 652434 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[O:11][CH2:10][C:9](=[O:12])[CH:8]([C:13]([O:15][CH3:16])=[O:14])[S:7][C:6]=2[CH:17]=1.Br[CH2:19][CH2:20][CH2:21][Cl:22]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[O:11][CH2:10][C:9](=[O:12])[C:8]([CH2:19][CH2:20][CH2:21][Cl:22])([C:13]([O:15][CH3:16])=[O:14])[S:7][C:6]=2[CH:17]=1

Participants

3

Reactant 2

HCID 80061-Bromo-3-chloropropaneHCID 13536191HCID 13536191, compound

Product 1

HCID 13808542HCID 13808542, compound

Procedure

Methyl 7-chloro-3-oxo-3,4-dihydro-2H-1,5-benzoxathiepin-4-carboxylate is treated with 1-bromo-3-chloropropane in the same manner as described in Reference Example 25 to give methyl 7-chloro-4-(3-chloropropyl)-3-oxo-3,4-dihydro-2H-1,5-benzoxathiepin-4-carboxylate as a colorless oil.

Sources & evidence

ORD record
ord-187bd3524ce244db91a56e40dc2e3726
Source dataset
uspto-grants-1987_06
Patent number
US04672064

Reaction notes

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