HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → HCID 12803197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | HCID 12803194 | HCID 12803194 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12803197 | HCID 12803197 | — |
Reaction Steps
A mixture of phenylmethyl [2-[5-(aminomethyl)-1H-indol-3-yl]ethyl]carbamate (0.25 g), ethyl formate (5 ml) and ethanol (1 ml) was heated under reflux for 9 h. The solvent was evaporated in vacuo and the residue was evaporated with ethanol (2×5 ml) to give the title compound (0.27 g) as cream crystals m.p. 114°-6°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672067 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-7a92483a4bc642d295f856d442038cfa |
| Source note | uspto-grants-1987_06 |