HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → HCID 12822524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | Acetryptine | HCID 20810 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12822524 | HCID 12822524 | — |
Reaction Steps
A suspension of 5-acetyl-1H-indole-3-ethanamine (1.0 g), phthalic anhydride (0.83 g) and sodium acetate (1.0 g) in acetic acid (15 ml) was heated at reflux for 3 h. On cooling the title compound was deposited as an off-white crystalline solid (1.5 g) m.p. 234°-5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672067 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-d50701c0ce8a47deaf2f43b358718739 |
| Source note | uspto-grants-1987_06 |