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HRID652481

反应详情

EQUATION

反应方程式

HRID 652481 的结构方程式

REACTANTS

反应物

2
结构：NCCCc1cccnc1
HCID13557523

3-(Pyridin-3-yl)propan-1-amine

C8H12N2

结构：CCCc1c(OCCCC(=O)O)ccc(C(C)=O)c1O
HCID13753871

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1c(OCCCC(=O)NCCCc2cccnc2)ccc(C(C)=O)c1O
HCID13912782

未命名化合物

PROCEDURE

实验过程

4-(4-Acetyl-3-hydroxy-2-propylphenoxy)butanoic acid was allowed to react with 3-pyridine propanamine according to procedure A and the product was purified by chromatography on silica gel to give 4-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[3-(3-pyridinyl)propyl]butanamide, the title compound, mp 97°-98° (from methylene chloride-ether) in 88% yield.

WORKUP

后处理

  1. customthe product was purified by chromatography on silica gel