huagongshe.com
HRID652484

反应详情

EQUATION

反应方程式

HRID 652484 的结构方程式

REACTANTS

反应物

2
结构：NCCCCc1cncnc1
HCID13557543

5-Pyrimidinebutanamine

C8H13N3

结构：CCCc1c(OCCCCCC(=O)O)ccc(C(C)=O)c1O
HCID13753873

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1c(OCCCCCC(=O)NCCCCc2cncnc2)ccc(C(C)=O)c1O
HCID13912776

未命名化合物

PROCEDURE

实验过程

6-(4-Acetyl-3-hydroxy-2-propylphenoxy)hexanoic acid was allowed to react with 5-pyrimidine butanamine according to procedure A and the product was purified by crystallization from carbon tetrachloride to give 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(5-pyrimidinyl)-butyl]hexanamide, the title compound mp 87°-89°, in 73% yield.

WORKUP

后处理

  1. customthe product was purified by crystallization from carbon tetrachloride