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HRID652485

反应详情

EQUATION

反应方程式

HRID 652485 的结构方程式

REACTANTS

反应物

2
结构：NCCSc1ccncc1
HCID13557535

未命名化合物

结构：CCCc1c(OCCCCCC(=O)O)ccc(C(C)=O)c1O
HCID13753873

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1c(OCCCCCC(=O)NCCSc2ccncc2)ccc(C(C)=O)c1O
HCID13912777

未命名化合物

PROCEDURE

实验过程

6-(4-Acetyl-3-hydroxy-2-propylphenoxy)hexanoic acid was allowed to react with 2-(4-pyridinylthio)ethyl amine according to procedure A and the product was purified by crystallization from ethyl acetate-hexane to give 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[2-(4-pyridinylthio)ethyl]hexanamide, the title compound, mp 63°-65°, in 52% yield.

WORKUP

后处理

  1. customthe product was purified by crystallization from ethyl acetate-hexane