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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 65251Erstellt: 25. Oktober 2026

1-Methylimidazole → HCID 178480862, Verbindung

https://huagongshe.com/reaction/65251

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-MethylimidazoleHCID 1390—
Edukt1-Chloro-4-(4-chlorobutyl)benzeneHCID 20082732—
ProduktHCID 178480862HCID 178480862—

Reaktionsschritte

Combine 6.1 g (0.03 mole) 1-chloro-4-(4-chlorobutyl)benzene with 2.5 g (0.03 mole) 1-methyl-1H-imidazole and heat at 120° C., following the course of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5). At the completion of the reaction, cool and triturate with ether, collect the solid and recrystallize from 50 ml hot acetone to obtain the title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04613609
Quelldatensatzuspto-grants-1986_09
ORD IDord-789f015a518643958156a7ed367e7d7e
Quellennotizuspto-grants-1986_09