HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 3-[(4-Acetyl-3-hydroxy-2-propylphenoxy)methyl]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-[(4-Acetyl-3-hydroxy-2-propylphenoxy)methyl]benzoic acid methyl ester | HCID 13912817 | — |
| Product | 3-[(4-Acetyl-3-hydroxy-2-propylphenoxy)methyl]benzoic acid | HCID 13912816 | — |
Reaction Steps
3-[(4-Acetyl-3-hydroxy-2-propylphenoxy)methyl]benzoic acid methyl ester was allowed to react with 1.0N sodium hydroxide according to the procedure of Example 70 and the product was purified by recrystallization from acetone to give 3-[(4-acetyl-3-hydroxy-2-propylphenoxy)methyl]benzoic acid, the title compound, m.p. 221°-224°, in 92% yield. Analysis Calculated for C19H20O5 : C, 69.50; H, 6.14. Found: C, 69.64; H, 6.35.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672066 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-42ad1c718576426aaec8dd993239965f |
| Source note | uspto-grants-1987_06 |