HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-(bromomethyl)benzoate → Methyl Benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-(bromomethyl)benzoate | HCID 2734813 | — |
| Reactant | 2',4'-Dihydroxy-3'-propylacetophenone | HCID 2775198 | — |
| Product | Methyl Benzoate | HCID 7150 | — |
Reaction Steps
1-(2,4-dihydroxy-3-propylphenyl)ethanone was allowed to react with methyl 2-bromomethylbenzoate according to the procedure of Example 69 and the product was purified by recrystallization from hexane to give 2-[4-acetyl-3-hydroxy-2-propylphenoxy)methyl]benzoic acid methyl ester, the title compound, m.p. 90°-93°, in 78% yield. Analysis Calculated for C20H22O5 : C, 70.16, H, 6.48. Found: C, 69.97; H, 6.36.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672066 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-4a6426ca68844ec58f249ac671688d4d |
| Source note | uspto-grants-1987_06 |