huagongshe.com
HRID652523

反应详情

EQUATION

反应方程式

HRID 652523 的结构方程式

REACTANTS

反应物

2
结构：CCCc1c(O)ccc(C(C)=O)c1O
HCID2775198

1-(2,4-Dihydroxy-3-propylphenyl)ethan-1-one

C11H14O3

结构：CCOC(=O)c1ccc(CBr)cc1OCC
HCID10589339

Benzoic acid, 4-(bromomethyl)-2-ethoxy-, ethyl ester

C12H15BrO3

PRODUCTS

生成物

1
结构：CCCc1c(OCc2ccc(C(=O)OCC)c(OCC)c2)ccc(C(C)=O)c1O
HCID13912822

未命名化合物

PROCEDURE

实验过程

1-(2,4-dihydroxy-3-propylphenyl)ethanone was allowed to react with 4-(bromomethyl)-2-ethoxybenzoic acid ethyl ester according to the procedure of Example 69 and the product was purified by HPLC to give 4-[(4-acetyl-3-hydroxy-2-propylphenoxy)methyl]-2-ethoxybenzoic acid ethyl ester, the title compound, m.p. 92°-94° in 83% yield.

WORKUP

后处理

  1. customthe product was purified by HPLC