HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride, 3-chloro- → 106106-52-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Reactant | 2-Amino-5-methylbenzoic acid | HCID 76255 | — |
| Product | 106106-52-9 | HCID 317080 | 91.1% |
Reaction Steps
When the reaction conditions of Example 1 are employed but 11.3 g of 5-methylanthranilic acid and 13.1 g of 3-chlorobenzoyl chloride are used, 18.5 g (91%) of 6-methyl-2-(m-chlorophenyl)-4H-3,1-benzoxazin-4-one of melting point 160°-162° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04673740 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-58edeff5b5eb461c9becc0d5c12e6111 |
| Source note | uspto-grants-1987_06 |