HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 136393678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | (2,3-Dichloro-4-hydroxyphenyl)(phenyl)methanone | HCID 14009997 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 136393678 | HCID 136393678 | — |
Reaction Steps
A solution of 18.0 g of 2,3-dichloro-4-hydroxybenzophenone and 9.3 g of hydroxylamine hydrochloride in 100 ml of pyridine is refluxed for 2 hours. Thereafter, the pyridine is evaporated under vacuum and the residual liquid is partitioned between 5% hydrochloric acid and ethyl acetate. The ethylacetate extract is washed with water, dried, and evaporated to give 2,3-dichloro-4-hydroxy-benzophenone oxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04673746 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-6f02e04d363742f19abd1a1c2261cdb1 |
| Source note | uspto-grants-1987_06 |