HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 652880Generated: October 25, 2026
Pyridinium chloride → 2,3-Dichloro-4-hydroxy-4'-fluorobenzophenone
https://huagongshe.com/reaction/652880
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 2,3-Dichloro-4-methoxy-4'-fluorobenzophenone | HCID 20150631 | — |
| Product | 2,3-Dichloro-4-hydroxy-4'-fluorobenzophenone | HCID 13015707 | — |
Reaction Steps
A mixture of 39.5 g of 2,3-dichloro-4-methoxy-4'-fluorobenzophenone and 160 g of pyridine hydrochloride is heated at 200° C. for one hour. The reaction mixture is poured into ice water with stirring and a precipitate forms. The precipitate is filtered and dried for about 18 hours to yield 2,3-dichloro-4-hydroxy-4'-fluorobenzophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04673746 |
|---|
| Source dataset | uspto-grants-1987_06 |
|---|
| ORD ID | ord-6befd78396e1408d834f837ba11e8b56 |
|---|
| Source note | uspto-grants-1987_06 |
|---|
