HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-1,2-propanediol → HCID 86151647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-1,2-propanediol | HCID 7290 | — |
| Reactant | 3,3'-(Butylazanediyl)di(propane-1,2-diol) | HCID 6455201 | — |
| Product | HCID 86151647 | HCID 86151647 | — |
Reaction Steps
A fresh quantity of 66.3 g (0.6 mole) of 1-chloro-2,3-propanediol was added to the unpurified bis(2,3-dihydroxypropyl)-n-butylamine. These reagents were then brought to a temperature of 100° C. for 26 hours. Separation of the ammonium salt form was carried out in a methanolic medium with the aid of a cation exchange resin (Bio-Rad AG 50W-X8). In this way, 21.9 g of n-butyl-tris(2,3-dihydroxypropyl)ammonium chloride were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675131 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-da2926ec961341b7ac72af209ab1687d |
| Source note | uspto-grants-1987_06 |