HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 4H-1,2,4-Triazole, 3-methyl-5-(methylthio)-4-phenyl- | HCID 1143246 | — |
| Product | HCID 178503614 | HCID 178503614 | — |
Reaction Steps
Then, 10 g of 5 methyl-3-methylthio-4-phenyl-1,2,4-triazole thus obtained was mixed with 40 g of methyl iodide and the mixture was heat-refluxed for 4 hours to precipitate crystals, which were collected by filtration and recrystallized from ethanol to provide 1,5-dimethyl-3-methylthio-4-phenyl-1,2,4-triazolium iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675276 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-db64228d94d742c1923662bd00d1d4a0 |
| Source note | uspto-grants-1987_06 |