HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 2768148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 12186839 | HCID 12186839 | — |
| Product | HCID 2768148 | HCID 2768148 | — |
Reaction Steps
Utilizing the general procedure of Example 2 and starting with benzaldehyde, thiourea and ethyl acetoacetate, ethyl 4-phenyl-3,4-dihydropyrimidine-2(1H)thione-5-carboxylate was prepared and then acylated with acetic anhydride to afford the title product as a solid (mp 142°-5° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675321 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-441a75bcb4de46bc9cef1e2ed70832ed |
| Source note | uspto-grants-1987_06 |