反应详情

To 28.9 g (0.2 mole) the p-chlorothiophenol and 8.0 g (0.2 mole) of sodium hydroxide in 100 ml of water is added 22.0 g (0.22 mole) of 1,2-epoxyhexane over 10 minutes. When addition is completed, the mixture is heated to reflux for 16 hours. The mixture is cooled, combined with 300 ml of water and the organic phase is separated.

1. additionWhen addition
2. temperaturethe mixture is heated
3. temperatureto reflux for 16 hours
4. temperatureThe mixture is cooled
5. customthe organic phase is separated