HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorothiophenol → HCID 13937443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Butyloxirane | HCID 15036 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13937443 | HCID 13937443 | — |
Reaction Steps
To 28.9 g (0.2 mole) the p-chlorothiophenol and 8.0 g (0.2 mole) of sodium hydroxide in 100 ml of water is added 22.0 g (0.22 mole) of 1,2-epoxyhexane over 10 minutes. When addition is completed, the mixture is heated to reflux for 16 hours. The mixture is cooled, combined with 300 ml of water and the organic phase is separated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675316 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-b1f9d12b79824e34be609eba70338d45 |
| Source note | uspto-grants-1987_06 |