HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 13382702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 4-phenylsulfanylbutanenitrile | HCID 271501 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13382702 | HCID 13382702 | 102.9% |
Reaction Steps
To a solution of 50 g (0.28 mole) of 4-phenylthiobutyronitrile in 200 ml of methylene chloride is added 40.5 g (0.3 mole) of sulfuryl chloride dropwise during a period of six hours. Stirring is continued overnight. Solvent and excess sulfuryl chloride is then evaporated under vacuum to give 61 g of a crude product. This material is used in the next experiment without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675316 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-c47a004dd6284f2babbf9e21b936bd50 |
| Source note | uspto-grants-1987_06 |