Potassium Iodide → HCID 20195590, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 1-chloro-3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propane (2.4 g) in dry acetonitrile (30 ml) was added potassium iodide (1.66 g), and triphenylphosphine (2.63 g) and the suspension heated at reflux for 24 hours. The cooled solution was filtered and the filtrate evaporated under reduced pressure to give a colourless oil which on cooling to -20° C. gave a white oily solid.

Provenance & Evidence