HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 9-(Methoxycarbonyl)-nonyl-triphenyl-phosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Methyl 10-bromodecanoate | HCID 554079 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 9-(Methoxycarbonyl)-nonyl-triphenyl-phosphonium bromide | HCID 10744695 | — |
Reaction Steps
A mixture of methyl-10bromodecanoate (5.22 g), triphenylphosphine (7.74 g) and sodium iodide (0.3 g) in acetonitrile (50 ml) was refluxed for 24 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675335 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-3718753e28e449c788e5d50ff67a1cd8 |
| Source note | uspto-grants-1987_06 |