Ethanol → HCID 53706224, compound

HRID 653109Notes

Reaction equation

BrC[C:3]1[CH:4]=[CH:5][C:6]2[O:10][C:9]([N+:11]([O-:13])=[O:12])=[C:8]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:7]=2[CH:20]=1.[NH:21]1[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1.[CH2:27](O)C>>[N+:11]([C:9]1[O:10][C:6]2[CH:5]=[CH:4][CH:3]=[C:20]([CH2:27][N:21]3[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]3)[C:7]=2[C:8]=1[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([O-:13])=[O:12]

Participants

Reactant 3

HCID 702Ethanol

HCID 8082Piperidine

HCID 13531604HCID 13531604, compound

Product 1

HCID 53706224HCID 53706224, compound

Procedure

Using the method of Example 6, 5-bromomethyl-2-nitro-3-phenylbenzofuran is reacted with piperidine in ethanol to provide N-(2-nitro-3-phenylbenzofuranylmethyl)piperidine having the structure ##STR37##

Sources & evidence

ORD record: ord-74c91171b152463d97d485811c375419
Source dataset: uspto-grants-1987_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04675320

Reaction notes

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