HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 178467032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 178418600 | HCID 178418600 | — |
| Reactant | HCID 178467031 | HCID 178467031 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178467032 | HCID 178467032 | 63.6% |
Reaction Steps
Prepared by the procedure described in Example 26 from 2.8 g (0.0074 mole) of 3-ethoxy-5-methoxy-1-phenyl-N-1H-tetrazol-5-yl-1H-indole-2-carboxamide and 1.3 g (0.0075 mole) of L-arginine, except that the solvent was ethanol rather than methanol. There was obtained 2.6 g (63% yield) of the arginine salt product, analytically pure containing 1.0 equivalent of water of hydration, mp 165° C.-dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675332 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-dc85671393274cc4bd01eb87fede3ef0 |
| Source note | uspto-grants-1987_06 |