Chloral Hydrate → HCID 57046400, compound

HRID 653191Notes

Reaction equation

HRID 653191 reaction equation
[Cl:1][C:2]([Cl:7])([Cl:6])[CH:3](O)O.[C:8]1([CH3:19])[CH:13]=[CH:12][C:11]([S:14]([NH:17][NH2:18])(=[O:16])=[O:15])=[CH:10][CH:9]=1>CO>[C:8]1([CH3:19])[CH:9]=[CH:10][C:11]([S:14]([NH:17][N:18]=[CH:3][C:2]([Cl:7])([Cl:6])[Cl:1])(=[O:15])=[O:16])=[CH:12][CH:13]=1

Participants

4

Reactant 2

HCID 2707Chloral HydrateHCID 15303P-Toluenesulfonylhydrazide

Product 1

HCID 57046400HCID 57046400, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In 20 ml of methanol were dissolved 3.98 g (24 mmole) of chloral hydrate and 3.72 g (20 mmole) of p-toluenesulfonylhydrazine, and the mixture was stirred at room temperature for 40 minutes to form trichloroacetaldehyde-p-toluenesulfonylhydrazone.

Sources & evidence

ORD record
ord-7bd7460f5edd46cfb4b71e9e4f278180
Source dataset
uspto-grants-1987_06
Patent number
US04675412

Reaction notes

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